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No, it won't. Two gases will not separate like that if they've been mixed. On the contrary, if you have two layers of gas they will eventually mix by diffusion.Not speaking from experience, but argon is extremely heavy gas and will rapidly settle. I imagine that if you are standing and adding argon to the suit, it will rapidly sink and air an be purge at the neck.
Besides, argon is only 40% denser than air: Gases - Specific Gravities