Phosphoric Acid for rust cleaning / inhibitor: Mixture and Procedure

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Just thought I’d update this thread with additional results. I’ve learned new lessons and wanted to share.

I cleaned four different tanks after hydro. I used the flash rust mixture: 1/3 cup filled to 1 gallon total. This volume of fluid filled a single tank up to near the opening when they were on their side. This was true for both LP75’s and HP120’s: even the larger tanks were mostly filled. I mixed up two gallons and did two tanks at a time.

I simply placed the tanks on their side and rotated them 1/8 of a turn every 2 minutes. I then followed the rinse and dry procedure outlined above.

Looking at them after pouring the solution out showed dark grey steel with a little sheen of orange. The solution was barely grey. After drying them, the steel was light grey, with a bit more orange. I’m not sure if the orange was more noticeable after drying, or if they rusted a bit during the dry process. I suspect the former: I’ve used this rinse and drying process before with less resulting orange.

I suspect that the issue might be the strength of the solution or the amount of dwell time. This is the first time I’ve used the “flash rust” solution. I think it’s too weak for great/fast results. As a comparison, I reused the solution for the second set of tanks and got a similar result (improved but not pristine), so I don’t think the acid was exhausted, just maybe not done yet.

Looking back over my previous notes, I did more like 30 minutes of dwell instead of the 16 I did today. And the original source of this process suggests 30-60 minutes of tumbling. Plus my previous attempt used a stronger mixture. So it’s probably not reasonable to expect the same results! :)

These are my personal tanks and they look better than any tank I’ve ever had straight from hydro, so I will use them as they are. In the future, though, I think I’ll step up to the mildly-rusty mix. I don’t have a tumbler, and babysitting these to rotate them every few minutes is annoying. I’d rather use a touch more acid and (hopefully) get better results without taking more time. But next time I’ll check them after 15 minutes and if I see a bit of orange I’ll know they’ll need more time. Patience is a virtue. :)

Also, some specifics on the drying process: I didn’t time it, but I found that it took 300 PSI of drying air (from an LP72) to go from warm, moist air to cool air. The tank was still warm at that point. I kept drying until the tank was not actively warm, which was another 100 PSI. My wild guess is that the air drying took between 2 and 3 minutes total.
 
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